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Issue 113, 2015
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Mild deuteration method of terminal alkynes in heavy water using reusable basic resin

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Abstract

The mild and efficient deuteration of terminal alkynes (mono-substituted alkynes) proceeded in the presence of a basic anion exchange resin, WA30, which is a polystyrene polymer bearing a tertiary amine residue on the aromatic nuclei, in heavy water (D2O) at room temperature. WA30 could be easily removed by a simple filtration and repeatedly reused.

Graphical abstract: Mild deuteration method of terminal alkynes in heavy water using reusable basic resin

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Article information


Submitted
15 Sep 2015
Accepted
22 Oct 2015
First published
23 Oct 2015

RSC Adv., 2015,5, 92954-92957
Article type
Communication
Author version available

Mild deuteration method of terminal alkynes in heavy water using reusable basic resin

T. Yamada, K. Park, Y. Monguchi, Y. Sawama and H. Sajiki, RSC Adv., 2015, 5, 92954
DOI: 10.1039/C5RA18921G

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