Issue 64, 2014

Non-catalytic dehydration of N,N′-diacetylchitobiose in high-temperature water

Abstract

Non-catalytic synthesis of 4-O-β-2-acetamido-2-deoxy-D-glucopyranosyl 2-acetamido-2,3-dideoxydidehydro-glucopyranose (GND) from chitin disaccharide, N,N′-diacetylchitobiose (GlcNAc)2, was achieved, with a maximum yield of 24.7% in high-temperature water at 120–220 °C and 25 MPa with a reaction time of 8–39 s.

Graphical abstract: Non-catalytic dehydration of N,N′-diacetylchitobiose in high-temperature water

Supplementary files

Article information

Article type
Paper
Submitted
27 Jun 2014
Accepted
28 Jul 2014
First published
28 Jul 2014

RSC Adv., 2014,4, 33651-33657

Author version available

Non-catalytic dehydration of N,N′-diacetylchitobiose in high-temperature water

M. Osada, K. Kikuta, K. Yoshida, K. Totani, M. Ogata and T. Usui, RSC Adv., 2014, 4, 33651 DOI: 10.1039/C4RA06319H

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