SCHEDULED MAINTENANCE
Nafion-TMS mediated Mukaiyama aldol reaction of silyl enol ethers with aldehydes, obtained from mild oxidation of alcohols with polymer supported perruthenate (PSP), yielded α,β-unsaturated ketones, which upon treatment with hydrazines allowed the clean synthesis of 4,5-dihydro-1H-pyrazoles.
F. Haunert, M. H. Bolli, B. Hinzen and S. V. Ley, J. Chem. Soc., Perkin Trans. 1, 1998, 2235 DOI: 10.1039/A803609H
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