SCHEDULED MAINTENANCE
A lipase-catalysed method for a large-scale preparation of both (R)-(ee 99%) and (S)-solketal (ee 94% after double resolution) has been described. Separation of the reaction products in the resolution mixture was achieved by extraction/distillation and the unwanted enantiomer was racemized and recycled.
E. Vänttinen and L. T. Kanerva, J. Chem. Soc., Perkin Trans. 1, 1994, 3459 DOI: 10.1039/P19940003459
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