Jump to main content
Jump to site search
PLANNED MAINTENANCE Close the message box

Scheduled maintenance work on Wednesday 27th March 2019 from 11:00 AM to 1:00 PM (GMT).

During this time our website performance may be temporarily affected. We apologise for any inconvenience this might cause and thank you for your patience.

Issue 0, 1985
Previous Article Next Article

Nuclear magnetic resonance studies of 1,6-linked disaccharides


The signals in the 13C n.m.r. spectra of all anomeric forms of the methyl glycosides of D-Glcp-(1→6)-D-Glcp and D-Glcp-(1→6)-D-Galp in water have been assigned. The chemical-shift differences obtained by comparison with relevant monosaccharide derivatives were used to calculate 13C n.m.r. spectra of oligo- and poly-saccharides containing 1,6-linkages. Good agreement between calculated and experimental spectra were obtained for raffinose, stachyose, dextran, and pustulan. The importance of comparing spectra determined at the same temperature is emphasized. Temperature shifts may, in favourable cases, be used for assignment of signals.

Back to tab navigation

Article type: Paper
DOI: 10.1039/P19850002383
Citation: J. Chem. Soc., Perkin Trans. 1, 1985,0, 2383-2388

  •   Request permissions

    Nuclear magnetic resonance studies of 1,6-linked disaccharides

    M. Forsgren, P. Jansson and L. Kenne, J. Chem. Soc., Perkin Trans. 1, 1985, 0, 2383
    DOI: 10.1039/P19850002383

Search articles by author