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Issue 39, 2012
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KI-catalyzed imidation of sp3 C–H bond adjacent to amidenitrogen atom

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Abstract

We have developed a new KI-catalyzed method for the imidation of an sp3 C–H bond adjacent to an amide nitrogen atom by using TBHP (tert-butyl hydroperoxide, 70% aqueous solution) as the oxidant. This novel procedure tolerated air and moisture and provided a series of novel products in moderate to excellent yields under mild conditions.

Graphical abstract: KI-catalyzed imidation of sp3 C–H bond adjacent to amide nitrogen atom

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Article information


Submitted
21 Jul 2012
Accepted
24 Aug 2012
First published
28 Aug 2012

Org. Biomol. Chem., 2012,10, 7869-7871
Article type
Communication

KI-catalyzed imidation of sp3 C–H bond adjacent to amide nitrogen atom

Z. Lao, W. Zhong, Q. Lou, Z. Li and X. Meng, Org. Biomol. Chem., 2012, 10, 7869
DOI: 10.1039/C2OB26430G

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