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Issue 24, 2010
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Total syntheses of the furanosesquiterpenes crassifolone and dihydrocrassifolone via an Au(i)-catalysed intramolecular Michael addition reaction

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Abstract

The racemic modifications of title natural products 1 and 2 have been synthesised for the first time. The key step was the Au(I)-catalysed conversion of the furanyl-substituted ynone 13 into the annulated furan 14.

Graphical abstract: Total syntheses of the furanosesquiterpenes crassifolone and dihydrocrassifolone via an Au(i)-catalysed intramolecular Michael addition reaction

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Article information


Submitted
26 Jul 2010
Accepted
13 Sep 2010
First published
07 Oct 2010

Org. Biomol. Chem., 2010,8, 5483-5485
Article type
Communication

Total syntheses of the furanosesquiterpenes crassifolone and dihydrocrassifolone via an Au(I)-catalysed intramolecular Michael addition reaction

R. S. Menon and M. G. Banwell, Org. Biomol. Chem., 2010, 8, 5483
DOI: 10.1039/C0OB00487A

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