Attempted reduction of 1,2,3-thiadiazole-4-carboxylates with samarium/iodine in methanol. Unexpected ring enlargement to 1,2,5-trithiepan-4,6-dicarboxylates
Abstract
When stirred with powdered samarium and iodine in
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* Corresponding authors
a Core Research for Evolutional Science and Technology (CREST), Japan Science and Technology Corporation (JST), Kawaguchi, Japan
b
Department of Chemistry, School of Science, Kwansei Gakuin University, Gakuen 2-1, Sanda, Japan
E-mail:
hsuzuki@ksc.kwansei.ac.jp
c
Department of Mathematical and Life Sciences, Graduate School of Science, Hiroshima University, Higashi-Hiroshima, Japan
E-mail:
hmorikawa@sci.hiroshima-u.ac.jp
When stirred with powdered samarium and iodine in
K. Miyawaki, H. Suzuki and H. Morikawa, Org. Biomol. Chem., 2004, 2, 2870 DOI: 10.1039/B408195A
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