Issue 3, 2005
From the journal:

New Journal of Chemistry

Polymorphism in nickel phosphonates: synthesis of layered and microporous Ni(O3PCH2C(O)NH2)·H2O

Rakesh Modi,a   Gary B. Hix,*a   Maryjane Tremayneb  and  Elizabeth MacLeanc  

* Corresponding authors

a Leicester School of Pharmacy, De Montfort University, The Gateway, Leicester, UK
E-mail: ghix@dmu.ac.uk

b The School of Chemistry, University of Birmingham, Edgbaston, Birmingham, UK

c CCLRC Daresbury Laboratory, Daresbury, Warrington, Cheshire, UK

Abstract

Two new polymorphic nickel phosphonates have been prepared by a reaction between nickel acetate and diethyl cyanomethylphosphonate. The acidity of the nickel solution affects the hydrolysis of the phosphonate to produce the phosphonic acid in situ.

Graphical abstract: Polymorphism in nickel phosphonates: synthesis of layered and microporous Ni(O3PCH2C(O)NH2)·H2O

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Article information

DOI
https://doi.org/10.1039/B411740A
Article type
Letter
Submitted
30 Jul 2004
Accepted
10 Jan 2005
First published
27 Jan 2005

New J. Chem., 2005,29, 427-429

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Polymorphism in nickel phosphonates: synthesis of layered and microporous Ni(O3PCH2C(O)NH2)·H2O

R. Modi, G. B. Hix, M. Tremayne and E. MacLean, New J. Chem., 2005, 29, 427 DOI: 10.1039/B411740A

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