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Issue 6, 2002
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A novel synthesis approach to transition metal boracites

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Abstract

Five halogen boracites, Mn3B7O13Cl, Co3B7O13Cl, Ni3B7O13Cl, Cu3B7O13Cl, Zn3B7O13I, have been synthesized by reaction of transition metal halides and boric acid at low temperature in the flux of boric acid. X-ray powder diffraction and chemical analysis of the halogen content show that the products are indeed stoichiometric halogen boracites, indicating that the proposed synthesis procedure is a convenient and promising way to the halogen boracites.

Graphical abstract: A novel synthesis approach to transition metal boracites

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Publication details

The article was received on 17 Oct 2001, accepted on 13 Feb 2002 and first published on 15 Apr 2002


Article type: Paper
DOI: 10.1039/B109461K
J. Mater. Chem., 2002,12, 1771-1774

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    A novel synthesis approach to transition metal boracites

    J. Ju, H. Li, Y. Wang, J. Lin and C. Dong, J. Mater. Chem., 2002, 12, 1771
    DOI: 10.1039/B109461K

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