Issue 10, 2014
From the journal:

Journal of Analytical Atomic Spectrometry

Fast determination of the surface density of titanium in ultrathin layers using LIBS spectrometry

Tomáš Kratochvíl,a   Tomáš Černohorský,*a   Petr Knotek,b   Lukáš Kalina,c   Jakub Návesník,a   Miloslav Pouzara  and  Magdalena Zvolskáa  

* Corresponding authors

a University of Pardubice, Institute of Environmental and Chemical Engineering, Studentska 573, 532 10 Pardubice, Czech Republic
E-mail: tomas.cernohorsky@upce.cz

b University of Pardubice, Faculty of Chemical Technology, Joint Laboratory of Solid State Chemistry of IMC and University of Pardubice, Studentska 573, 532 10 Pardubice, Czech Republic

c Brno University of Technology, Faculty of Chemistry, Centre for Materials Research CZ.1.05/2.1.00/01.0012, Purkyňova 464/118, Brno, CZ-612 00, Czech Republic

Abstract

This work deals with the use of laser-induced breakdown spectroscopy (LIBS) for determining the surface density of titanium in ultrathin layers, particularly in ultrathin layers on a steel sheet. The results obtained by LIBS spectroscopy were compared with those obtained by wavelength dispersive X-ray fluorescence spectroscopy (WDXRF), X-ray photoelectron spectroscopy (XPS) and laser ablation inductively coupled plasma time of flight mass spectrometry (LA-ICP-TOF-MS). A simple, cheap and efficient method for the determination of the surface density of titanium in thin layers has been developed.

Graphical abstract: Fast determination of the surface density of titanium in ultrathin layers using LIBS spectrometry

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Article information

DOI
https://doi.org/10.1039/C3JA50398D
Article type
Paper
Submitted
20 Dec 2013
Accepted
26 Jun 2014
First published
26 Jun 2014
This article is Open Access
Creative Commons BY-NC license

J. Anal. At. Spectrom., 2014,29, 1806-1812

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Fast determination of the surface density of titanium in ultrathin layers using LIBS spectrometry

T. Kratochvíl, T. Černohorský, P. Knotek, L. Kalina, J. Návesník, M. Pouzar and M. Zvolská, J. Anal. At. Spectrom., 2014, 29, 1806 DOI: 10.1039/C3JA50398D

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