Issue 44, 2013
From the journal:

Dalton Transactions

Recent developments in the synthetic chemistry of technetium disulfide†

Maryline Ferrier,*a   William M. Kerlin,a   Frederic Poineau,a   Alfred P. Sattelbergerab  and  Kenneth R. Czerwinskia  

* Corresponding authors

a Department of Chemistry, University of Nevada Las Vegas, 4505 S. Maryland Parkway Box 454009, Las Vegas, NV 89154-4009, USA
E-mail: maryline.ferrier@gmail.com
Tel: (+1)-702-895-5517

b Energy Engineering and Systems Analysis Directorate, Argonne National Laboratory, Argonne, IL 60439, USA

Abstract

Technetium disulfide was prepared by reaction between the elements in a sealed tube at 450 °C, by reaction between Tc2(O2CCH3)5 and H2S gas in a flowing system at 450 °C and by reaction between K2TcCl6 and H2S gas in sulfuric acid. The samples were analysed by X-ray absorption fine structure (XAFS) spectroscopy.

Graphical abstract: Recent developments in the synthetic chemistry of technetium disulfide

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Article information

DOI
https://doi.org/10.1039/C3DT52079J
Article type
Communication
Submitted
01 Aug 2013
Accepted
12 Sep 2013
First published
17 Sep 2013

Dalton Trans., 2013,42, 15540-15543

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Recent developments in the synthetic chemistry of technetium disulfide

M. Ferrier, W. M. Kerlin, F. Poineau, A. P. Sattelberger and K. R. Czerwinski, Dalton Trans., 2013, 42, 15540 DOI: 10.1039/C3DT52079J

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