Issue 4, 2012

Palladium(ii)–selenoether complexes as new single source precursors: First synthesis of Pd4Se and Pd7Se4 nanoparticles

Abstract

Pd4Se and Pd7Se4 nanoparticles (size 38–104 nm), protected by TOP, have been obtained for the first time using Pd(II) ligated with selenated primary and secondary amines (see 1 and 2) as single source precursors respectively. TEM, SEM, powder XRD and photoluminescence have been used to characterize them. 1 and 2 are also the first Pd(II)–selenoether complexes used for the synthesis of nanoparticles containing palladium and selenium.

Graphical abstract: Palladium(ii)–selenoether complexes as new single source precursors: First synthesis of Pd4Se and Pd7Se4 nanoparticles

Supplementary files

Article information

Article type
Communication
Submitted
04 Nov 2011
Accepted
22 Nov 2011
First published
12 Dec 2011

Dalton Trans., 2012,41, 1142-1145

Palladium(II)–selenoether complexes as new single source precursors: First synthesis of Pd4Se and Pd7Se4 nanoparticles

V. V. Singh, G. K. Rao, A. Kumar and A. K. Singh, Dalton Trans., 2012, 41, 1142 DOI: 10.1039/C2DT12113A

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