Hydrothermal synthesis and structural characterization of the first mixed molybdenum–tungsten capped-keggin polyoxometal complex: {[Co(dien)]4[(AsVO4)MoV8WVI4O33(µ2–OH)3]}·2H2O

Hai-Hui Yu; Xiao-Bing Cui; Ji-Wen Cui; Li Kong; Wei-Jie Duan; Ji-Qing Xu; Tie-Gang Wang

doi:10.1039/B711604G

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Hydrothermal synthesis and structural characterization of the first mixed molybdenum–tungsten capped-keggin polyoxometal complex: {[Co(dien)]₄[(As^VO₄)Mo^V₈W^VI₄O₃₃(µ₂–OH)₃]}·2H₂O†

Hai-Hui Yu,^a Xiao-Bing Cui,^a Ji-Wen Cui,^ab Li Kong,^c Wei-Jie Duan,^a Ji-Qing Xu*^a and Tie-Gang Wang^a

Author affiliations

* Corresponding authors

^a College of Chemistry and State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun, PR China

^b College of Chemistry and Pharmacy, Jiamusi University, Jiamusi, PR China

^c College of Chemistry Jilin University, Changchun, PR China
E-mail: xjq@mail.jlu.edu.cn
Fax: +86 431 88499158
Tel: +86 431 88499132

Abstract

The first polyoxometal complex possessing affirmatory mixed molybdenum–tungsten capped Keggin-type structure has been hydrothermally synthesized.

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Supplementary files

Crystal structure data TXT (37K)

Article information

DOI: https://doi.org/10.1039/B711604G
Article type: Communication
Submitted: 15 Aug 2007
Accepted: 11 Oct 2007
First published: 19 Oct 2007

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Dalton Trans., 2008, 195-197

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Hydrothermal synthesis and structural characterization of the first mixed molybdenum–tungsten capped-keggin polyoxometal complex: {[Co(dien)]₄[(As^VO₄)Mo^V₈W^VI₄O₃₃(µ₂–OH)₃]}·2H₂O

H. Yu, X. Cui, J. Cui, L. Kong, W. Duan, J. Xu and T. Wang, Dalton Trans., 2008, 195 DOI: 10.1039/B711604G

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Dalton Transactions