SCHEDULED MAINTENANCE
The reductive cyclisation of 3-chloropropyliodo(methyl)arsine and 3-chloropropyliodo(phenyl)arsine with sodium in tetrahydrofuran affords the four-membered alicyclic tertiary arsines 1-methylarsetan and 1-phenylarsetan respectively. The five-membered homologues 1-methyl- and 1-phenyl-arsolan may be prepared similarly from the corresponding 4-chlorobutyliodo-methylarsine and -phenylarsine.
M. Mickiewicz and S. B. Wild, J. Chem. Soc., Dalton Trans., 1977, 704 DOI: 10.1039/DT9770000704
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