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Issue 1, 2011
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High-resolution solid-state 13C μMAS NMR with long coherence life times

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Abstract

Longer coherence life times (i.e. smaller homogeneous linewidths) can be achieved for carbon resonances which are strongly coupled to protons with high rf field heteronuclear decoupling in micro magic angle spinning NMR. Better proton decoupling enhances the sensitivity and resolution of two-dimensional through-bond correlation experiments for mass-limited samples with uniform carbon labeling.

Graphical abstract: High-resolution solid-state 13C μMAS NMR with long coherence life times

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Publication details

The article was received on 24 Sep 2010, accepted on 18 Oct 2010 and first published on 12 Nov 2010


Article type: Communication
DOI: 10.1039/C0CP01929A
Phys. Chem. Chem. Phys., 2011,13, 104-106

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    High-resolution solid-state 13C μMAS NMR with long coherence life times

    S. K. Vasa, H. Janssen, E. R. H. Van Eck and A. P. M. Kentgens, Phys. Chem. Chem. Phys., 2011, 13, 104
    DOI: 10.1039/C0CP01929A

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