Issue 44, 2019

Quaternary ferrites by batch and continuous flow hydrothermal synthesis: a comparison

Abstract

Crystalline spinel quaternary ferrites MxZn1−xFe2O4 (M = Co, Ni; x = 0.2, 0.35, 0.5, 0.65, 0.8) were synthesised through conventional batch hydrothermal synthesis (HT) at 135 °C as well as via continuous flow hydrothermal synthesis (CHFS). The as prepared compounds were thoroughly characterised from a compositional (ICP-MS, XPS) and structural (XRD) point of view in order to compare the synthetic approaches and achieve a greater understanding of how the chosen approach influences the characteristics of the resulting spinel.

Graphical abstract: Quaternary ferrites by batch and continuous flow hydrothermal synthesis: a comparison

Supplementary files

Article information

Article type
Paper
Submitted
17 Sep 2019
Accepted
14 Oct 2019
First published
14 Oct 2019

CrystEngComm, 2019,21, 6801-6809

Quaternary ferrites by batch and continuous flow hydrothermal synthesis: a comparison

M. Bastianello, S. Diodati, N. Dengo, L. McCafferty, C. Footer, D. Badocco, P. Pastore, J. Darr and S. Gross, CrystEngComm, 2019, 21, 6801 DOI: 10.1039/C9CE01462D

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