Synthesis and characterization of multipod frameworks of Cu2O microcrystals and Cu7S4 hollow microcages

Hongdan Zhang; Ziqing Zhang; Benxian Li; Yingjie Hua; Chongtai Wang; Xudong Zhao; Xiaoyang Liu

doi:10.1039/C5CE00286A

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Synthesis and characterization of multipod frameworks of Cu₂O microcrystals and Cu₇S₄ hollow microcages†

Hongdan Zhang,^a Ziqing Zhang,^a Benxian Li,^b Yingjie Hua,^c Chongtai Wang,^c Xudong Zhao*^a and Xiaoyang Liu*^a

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* Corresponding authors

^a State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, College of Chemistry, Jilin University, 2699 Qianjin Street, Changchun 130012, PR China
E-mail: liuxy@jlu.edu.cn
Fax: (+86) 431-85168316
Tel: (+86) 431-85168316

^b College of Earth Science, Jilin University, Changchun 130061, PR China

^c School of Chemistry and Chemical Engineering, Hainan Normal University, Haikou, PR China

Abstract

A variety of multipod frameworks of Cu₂O microcrystals have been prepared through careful control of the ratios of n-butyl alcohol to water, and novel 14-pod Cu₂O frameworks are first reported. Moreover, template-assisted synthesis of multipod frameworks of Cu₇S₄ microcages using the obtained Cu₂O microcrystals as sacrificial templates is reported.

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Article information

DOI: https://doi.org/10.1039/C5CE00286A
Article type: Communication
Submitted: 07 Feb 2015
Accepted: 18 Mar 2015
First published: 02 Apr 2015

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CrystEngComm, 2015,17, 3908-3911

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Synthesis and characterization of multipod frameworks of Cu₂O microcrystals and Cu₇S₄ hollow microcages

H. Zhang, Z. Zhang, B. Li, Y. Hua, C. Wang, X. Zhao and X. Liu, CrystEngComm, 2015, 17, 3908 DOI: 10.1039/C5CE00286A

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