Dimeric self-association of an isophthalamide macrocycle in solution and the solid state

Christopher J. Serpell; Owen Thomas; Barbara Odell; Timothy D. W. Claridge; Ricky Chall; Amber L. Thompson; Paul D. Beer

doi:10.1039/C1CE05271C

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Dimeric self-association of an isophthalamide macrocycle in solution and the solid state†

Christopher J. Serpell,‡*^a Owen Thomas,^a Barbara Odell,^a Timothy D. W. Claridge,^a Ricky Chall,^a Amber L. Thompson^a and Paul D. Beer^a

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^a Chemistry Research Laboratory, Department of Chemistry, University of Oxford, Mansfield Road, Oxford, UK

Abstract

An isophthalamide macrocycle used in anion-templated interpenetrated structures is found to participate in dimeric self-assembly throughout eight different crystal forms. Analysis of these, in combination with solution-phase NMR studies, reveals the nature of the hydrogen-bonded self-association, yielding new perspectives and potential applications for the macrocycle system.

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DOI: https://doi.org/10.1039/C1CE05271C
Article type: Paper
Submitted: 01 Mar 2011
Accepted: 07 Apr 2011
First published: 04 May 2011

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CrystEngComm, 2011,13, 4586-4591

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Dimeric self-association of an isophthalamide macrocycle in solution and the solid state

C. J. Serpell, O. Thomas, B. Odell, T. D. W. Claridge, R. Chall, A. L. Thompson and P. D. Beer, CrystEngComm, 2011, 13, 4586 DOI: 10.1039/C1CE05271C

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Dimeric self-association of an isophthalamide macrocycle in solution and the solid state†

Abstract

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Dimeric self-association of an isophthalamide macrocycle in solution and the solid state

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