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Issue 9, 2007
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Structural changes in the crystal packing of highly hindered symmetrical vicinal bis-amides

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Abstract

The crystal structures of 1,4-bis(3,5-di-tert-butyl-2-hydroxybenzamido)butane (1) and 1,3-bis(3,5-di-tert-butyl-2-hydroxybenzamido)-2,2-dimethylpropane (2) have being characterized by single crystal X-ray diffraction. Their crystal packing is discussed in terms of the different interactions they exhibit. A brief discussion, based on hydrogen bonds, on the structural features of bis-(3,5-di-tert-butyl-2-hydroxybenzamide) compounds is carried out.

Graphical abstract: Structural changes in the crystal packing of highly hindered symmetrical vicinal bis-amides

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Article information


Submitted
04 Dec 2006
Accepted
20 Apr 2007
First published
17 May 2007

CrystEngComm, 2007,9, 746-752
Article type
Paper

Structural changes in the crystal packing of highly hindered symmetrical vicinal bis-amides

C. A. Jiménez, J. B. Belmar, F. S. Delgado, M. Julve and C. Ruiz-Pérez, CrystEngComm, 2007, 9, 746
DOI: 10.1039/B617605D

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