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Issue 9, 2007
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Structural changes in the crystal packing of highly hindered symmetrical vicinal bis-amides

Claudio A. Jiménez,*a   Julio B. Belmar,a   Fernando S. Delgado,bc   Miguel Julved  and  Catalina Ruiz-Pérezb  
Author affiliations

* Corresponding authors

a Dpto. Química Orgánica. Facultad de Ciencias Químicas. Universidad de Concepción. Casilla 160-C, Concepción, Chile
E-mail: cjimenez@udec.cl

b Laboratorio de Rayos X y Materiales Moleculares. Dpto. de Física Fundamental II. Facultad de Física. Universidad de La Laguna. Avda. Astrofísico Francisco Sánchez s/n, 3820-La Laguna, Tenerife, Spain

c BM16 – LLS European Synchrotron Radiation Facility 6 Rue Jules Horowitz - BP 220 38043 Grenoble CEDEX 9, France

d ICMol/Departament de Química Inorgànica de la Universitat de València, Polígono La Coma s/n, 46980 Paterna (València), Spain

Abstract

The crystal structures of 1,4-bis(3,5-di-tert-butyl-2-hydroxybenzamido)butane (1) and 1,3-bis(3,5-di-tert-butyl-2-hydroxybenzamido)-2,2-dimethylpropane (2) have being characterized by single crystal X-ray diffraction. Their crystal packing is discussed in terms of the different interactions they exhibit. A brief discussion, based on hydrogen bonds, on the structural features of bis-(3,5-di-tert-butyl-2-hydroxybenzamide) compounds is carried out.

Graphical abstract: Structural changes in the crystal packing of highly hindered symmetrical vicinal bis-amides

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Publication details

The article was received on 04 Dec 2006, accepted on 20 Apr 2007 and first published on 17 May 2007


Article type: Paper
DOI: 10.1039/B617605D
CrystEngComm, 2007,9, 746-752

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    Structural changes in the crystal packing of highly hindered symmetrical vicinal bis-amides

    C. A. Jiménez, J. B. Belmar, F. S. Delgado, M. Julve and C. Ruiz-Pérez, CrystEngComm, 2007, 9, 746
    DOI: 10.1039/B617605D

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