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Issue 64, 2019
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Palladium-catalyzed decarbonylative annulation of phthalimides with arynes: direct construction of phenanthridinones

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Abstract

A novel palladium-catalyzed decarbonylative annulation for the synthesis of phenanthridinones from phthalimides and arynes has been developed. This catalytic system tolerates a broad range of functional groups. Mechanistic experiments demonstrate that the Pd(II) complex B is the key intermediate, which has been confirmed by X-ray crystallography for the first time.

Graphical abstract: Palladium-catalyzed decarbonylative annulation of phthalimides with arynes: direct construction of phenanthridinones

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Publication details

The article was received on 25 Jun 2019, accepted on 14 Jul 2019 and first published on 15 Jul 2019


Article type: Communication
DOI: 10.1039/C9CC04868E
Chem. Commun., 2019,55, 9507-9510

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    Palladium-catalyzed decarbonylative annulation of phthalimides with arynes: direct construction of phenanthridinones

    Y. Meng, X. Si, Y. Song, H. Zhou and F. Xu, Chem. Commun., 2019, 55, 9507
    DOI: 10.1039/C9CC04868E

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