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Issue 86, 2016

Pd-Supported on N-doped carbon: improved heterogeneous catalyst for base-free alkoxycarbonylation of aryl iodides

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Abstract

Novel Pd-based heterogeneous catalysts were prepared through immobilization of Pd(OAc)2/phenanthroline on carbon and subsequent pyrolysis. The most active catalyst was characterized by TEM, XPS and XRD techniques and was successfully used for the base-free methoxycarbonylation of aryl iodides. Notably, no metal contamination (detection limit < 0.5 ppm) in the final products was observed.

Graphical abstract: Pd-Supported on N-doped carbon: improved heterogeneous catalyst for base-free alkoxycarbonylation of aryl iodides

Supplementary files

Article information


Submitted
06 Sep 2016
Accepted
04 Oct 2016
First published
04 Oct 2016

Chem. Commun., 2016,52, 12729-12732
Article type
Communication

Pd-Supported on N-doped carbon: improved heterogeneous catalyst for base-free alkoxycarbonylation of aryl iodides

I. Ziccarelli, H. Neumann, C. Kreyenschulte, B. Gabriele and M. Beller, Chem. Commun., 2016, 52, 12729 DOI: 10.1039/C6CC07269K

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