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Issue 84, 2015
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Measuring couplings in crowded NMR spectra: pure shift NMR with multiplet analysis

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Abstract

The PSYCHE method for pure shift NMR is exploited to generate 2D J spectra with full decoupling in one dimension and multiplet structure in the other, allowing spin–spin coupling constants to be measured even in very crowded spectra. Significant improvements over existing techniques are demonstrated for the hormones estradiol and androstenedione.

Graphical abstract: Measuring couplings in crowded NMR spectra: pure shift NMR with multiplet analysis

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Publication details

The article was received on 28 Jul 2015, accepted on 27 Aug 2015 and first published on 27 Aug 2015


Article type: Communication
DOI: 10.1039/C5CC06293D
Citation: Chem. Commun., 2015,51, 15410-15413
  • Open access: Creative Commons BY license
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    Measuring couplings in crowded NMR spectra: pure shift NMR with multiplet analysis

    M. Foroozandeh, R. W. Adams, P. Kiraly, M. Nilsson and G. A. Morris, Chem. Commun., 2015, 51, 15410
    DOI: 10.1039/C5CC06293D

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