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Issue 7, 2015
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Single-shot titrations and reaction monitoring by slice-selective NMR spectroscopy

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Abstract

A new method, based on slice-selective NMR spectroscopy of inhomogeneous mixtures, is introduced to perform NMR titrations and reaction monitoring in a single experiment. The method was applied to the titration of a lithium salt with 12-crown-4, and to the reaction of nBuLi with N,N,N′,N′′,N′′-pentamethyldiethylenetriamine (PMDTA).

Graphical abstract: Single-shot titrations and reaction monitoring by slice-selective NMR spectroscopy

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Supplementary files

Article information


Submitted
21 Oct 2014
Accepted
28 Nov 2014
First published
28 Nov 2014

This article is Open Access

Chem. Commun., 2015,51, 1275-1277
Article type
Communication
Author version available

Single-shot titrations and reaction monitoring by slice-selective NMR spectroscopy

T. Niklas, D. Stalke and M. John, Chem. Commun., 2015, 51, 1275
DOI: 10.1039/C4CC08329F

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