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Issue 86, 2013
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Pressure accelerated 1,3-dipolar cycloaddition of azide and alkyne groups in crystals

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Abstract

The cycloaddition of azides and alkynes in the solid state was accelerated by high pressure. In situ Raman scattering and synchrotron X-ray diffraction were employed to study reaction kinetics at different pressures which revealed that the pressure acceleration originates from the elevated substrate energy and decreased activation energy.

Graphical abstract: Pressure accelerated 1,3-dipolar cycloaddition of azide and alkyne groups in crystals

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Publication details

The article was received on 12 Aug 2013, accepted on 02 Sep 2013 and first published on 02 Sep 2013


Article type: Communication
DOI: 10.1039/C3CC46153J
Chem. Commun., 2013,49, 10130-10132

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    Pressure accelerated 1,3-dipolar cycloaddition of azide and alkyne groups in crystals

    B. Ni, K. Wang, Q. Yan, H. Chen, Y. Ma and B. Zou, Chem. Commun., 2013, 49, 10130
    DOI: 10.1039/C3CC46153J

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