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Issue 67, 2013
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The first general route for efficient synthesis of 18O labelled alcohols using the HOF·CH3CN complex

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Abstract

A mild and very efficient method for converting boronic acids to alcohols has been developed using the acetonitrile complex of hypofluorous acid HOF·CH3CN. Employing 18O-labeled water results in alcohols containing a heavy oxygen isotope. The reactions were performed at room temperature, within a few minutes and in excellent yields.

Graphical abstract: The first general route for efficient synthesis of 18O labelled alcohols using the HOF·CH3CN complex

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Supplementary files

Article information


Submitted
31 Mar 2013
Accepted
13 May 2013
First published
14 May 2013

Chem. Commun., 2013,49, 7379-7381
Article type
Communication

The first general route for efficient synthesis of 18O labelled alcohols using the HOF·CH3CN complex

J. Gatenyo, I. Vints and S. Rozen, Chem. Commun., 2013, 49, 7379
DOI: 10.1039/C3CC42337A

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