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Issue 68, 2012
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Total synthesis of (±)-pallambins C and D

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The first total synthesis of (±)-pallambins C and D has been accomplished in a linear 38 step reaction from (±)-Wieland–Miescher ketone. The key conversions are featured as follows: a Grob fragmentation–intramolecular aldol cyclization and a thiourea/palladium-catalyzed carbonylative annulation.

Graphical abstract: Total synthesis of (±)-pallambins C and D

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The article was received on 16 Jun 2012, accepted on 05 Jul 2012 and first published on 06 Jul 2012

Article type: Communication
DOI: 10.1039/C2CC34310J
Chem. Commun., 2012,48, 8517-8519

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    Total synthesis of (±)-pallambins C and D

    X. Xu, Z. Li, Y. Zhang, X. Peng and H. N. C. Wong, Chem. Commun., 2012, 48, 8517
    DOI: 10.1039/C2CC34310J

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