Issue 43, 2012
From the journal:

Chemical Communications

Efficient determination of diffusion coefficients by monitoring transport during recovery delays in NMR†

Rafal Augustyniak,abc   Fabien Ferrage,*abc   Christian Damblon,d   Geoffrey Bodenhausenabce  and  Philippe Pelupessyabc  

* Corresponding authors

a Ecole Normale Supérieure, Département de Chimie, 24 rue Lhomond, 75231 Paris Cedex 05, France
E-mail: Fabien.Ferrage@ens.fr

b Université Pierre et Marie Curie, Paris, France

c UMR 7203 Laboratoire des Biomolécules CNRS-UPMC-ENS, Paris, France

d Chimie Biologique Structurale, Institut de Chimie, Sart-Tilman (B6c), Université de Liège, 4000 Liège, Belgium

e Institut des Sciences et Ingénierie Chimiques, BCH, Ecole Polytechnique Fédérale de Lausanne, 1015 Lausanne, Switzerland

Abstract

A novel NMR approach allows one to efficiently determine translational diffusion coefficients of macromolecules in solution. This method for Signal Optimization with Recovery in Diffusion Delays (SORDID) monitors transport occurring during the recovery times between consecutive scans so that the duration of the measurements can be reduced approximately by a factor two.

Graphical abstract: Efficient determination of diffusion coefficients by monitoring transport during recovery delays in NMR

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Article information

DOI
https://doi.org/10.1039/C2CC30578J
Article type
Communication
Submitted
26 Jan 2012
Accepted
28 Mar 2012
First published
28 Mar 2012

Chem. Commun., 2012,48, 5307-5309

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Efficient determination of diffusion coefficients by monitoring transport during recovery delays in NMR

R. Augustyniak, F. Ferrage, C. Damblon, G. Bodenhausen and P. Pelupessy, Chem. Commun., 2012, 48, 5307 DOI: 10.1039/C2CC30578J

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