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Issue 26, 2012
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The dynamic chromatographic behavior of tri-o-thymotide on HPLC chiral stationary phases

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Abstract

The interconverting stereoisomers of tri-o-thymotide have been separated by HPLC on chiral stationary phases and the temperature dependence of the dynamic chromatographic patterns has been interpreted in terms of exchange between enantiomeric propeller and helical conformations. Computed low energy structures and CD spectra were used in absolute configuration assignment.

Graphical abstract: The dynamic chromatographic behavior of tri-o-thymotide on HPLC chiral stationary phases

  • This article is part of the themed collection: Chirality
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Article information


Submitted
02 Jan 2012
Accepted
04 Feb 2012
First published
06 Feb 2012

Chem. Commun., 2012,48, 3167-3169
Article type
Communication

The dynamic chromatographic behavior of tri-o-thymotide on HPLC chiral stationary phases

S. Levi Mortera, R. Sabia, M. Pierini, F. Gasparrini and C. Villani, Chem. Commun., 2012, 48, 3167
DOI: 10.1039/C2CC00021K

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