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Issue 7, 2011
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A convenient, high-sensitivity approach to multiple-resonance NMR at nanolitre volumes with inductively-coupled micro-coils

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Abstract

We propose using singly-tuned μ-coils and 1H-detection to obtain high-sensitivity in lieu of miniaturizing cumbersome multi-resonance circuits, with the existing MAS probe circuitry/coil providing RF at other frequencies. We demonstrate two key building blocks in solid-state NMR: cross-polarization and heteronuclear decoupling. As well, a 1H-detected 2D HMQC is obtained.

Graphical abstract: A convenient, high-sensitivity approach to multiple-resonance NMR at nanolitre volumes with inductively-coupled micro-coils

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Article information


Submitted
25 Oct 2010
Accepted
02 Dec 2010
First published
23 Dec 2010

Chem. Commun., 2011,47, 2119-2121
Article type
Communication

A convenient, high-sensitivity approach to multiple-resonance NMR at nanolitre volumes with inductively-coupled micro-coils

P. M. Aguiar, J. Jacquinot and D. Sakellariou, Chem. Commun., 2011, 47, 2119
DOI: 10.1039/C0CC04607H

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