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Issue 43, 2010
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Dynamic HPLC study of C70chlorination reveals a surprisingly selective synthesis of C70Cl8

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Abstract

A dynamic HPLC study of C70 chlorination led to the discovery, isolation, characterization, and development of the efficient preparatory procedures for two previously unknown soluble chlorofullerenes C70Cl8 and C70Cl6 and for insoluble [C70Cl8]n. A novel synthesis of 99% pure C70Cl10 with a nearly quantitative yield was also developed. The first stability study of C70Cl10,8,6 in solution showed that these compounds are very light-sensitive.

Graphical abstract: Dynamic HPLC study of C70 chlorination reveals a surprisingly selective synthesis of C70Cl8

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Article information


Submitted
09 Aug 2010
Accepted
03 Sep 2010
First published
27 Sep 2010

Chem. Commun., 2010,46, 8204-8206
Article type
Communication

Dynamic HPLC study of C70 chlorination reveals a surprisingly selective synthesis of C70Cl8

I. V. Kuvychko, A. A. Popov, A. V. Streletskii, L. C. Nye, T. Drewello, S. H. Strauss and O. V. Boltalina, Chem. Commun., 2010, 46, 8204
DOI: 10.1039/C0CC03134H

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