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Issue 32, 2010
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Monitoring the stepwise assembly of a 3-D framework from a supramolecular lanthanoid synthon by in situinfrared spectroscopy

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Abstract

Construction of a 3-D supramolecular network from [Ln(cpb)3(H2O)2] (Ln = Nd, Tb; Hcpb = 1-(4-cyanophenyl)-1,3-butanedione) by sequential displacement of a coordinated water by DMF, dimerisation by reciprocal hydrogen bonding in solution and π–π stacking and interdigitation of nitriles has been monitored by in situ fourier transform infrared spectroscopy.

Graphical abstract: Monitoring the stepwise assembly of a 3-D framework from a supramolecular lanthanoid synthon by in situ infrared spectroscopy

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Article information


Submitted
15 Apr 2010
Accepted
15 Jun 2010
First published
01 Jul 2010

Chem. Commun., 2010,46, 5948-5950
Article type
Communication

Monitoring the stepwise assembly of a 3-D framework from a supramolecular lanthanoid synthon by in situ infrared spectroscopy

P. C. Andrews, W. J. Gee, P. C. Junk, H. Krautscheid and J. G. MacLellan, Chem. Commun., 2010, 46, 5948
DOI: 10.1039/C0CC00949K

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