Issue 19, 2010
From the journal:

Chemical Communications

A robust, sensitive, and versatile HMBC experiment for rapid structure elucidation by NMR: IMPACT-HMBC†

Julien Furrer*a  

* Corresponding authors

a Service Analytique Facultaire, Institut of Chemistry, University of Neuchâtel, Avenue de Bellevaux 51, CH-2000 Neuchâtel, Switzerland
E-mail: julien.furrer@unine.ch
Fax: +4132 7182511
Tel: +4132 7182454

Abstract

A robust, versatile and easy to optimize HMBC experiment for complex organic structure elucidation which has been experimentally tested on cholesteryl acetate, cyclosporine and isopropylidene glycerol is described. The proposed experiment, IMPACT-HMBC (improved and accelerated constant-time heteronuclear multiple-bond correlation), combines sensitivity, easy experimental setup and can be recorded with short recovery times.

Graphical abstract: A robust, sensitive, and versatile HMBC experiment for rapid structure elucidation by NMR: IMPACT-HMBC

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Article information

DOI
https://doi.org/10.1039/C000964D
Article type
Communication
Submitted
14 Jan 2010
Accepted
10 Mar 2010
First published
01 Apr 2010

Chem. Commun., 2010,46, 3396-3398

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A robust, sensitive, and versatile HMBC experiment for rapid structure elucidation by NMR: IMPACT-HMBC

J. Furrer, Chem. Commun., 2010, 46, 3396 DOI: 10.1039/C000964D

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