Issue 8, 2009
From the journal:

Chemical Communications

High-precision heteronuclear 2D NMR experiments using 10-ppm spectral window to resolve carbon overlap†

Bruno Vitorge,a   Stefan Bieri,b   Munir Humam,b   Philippe Christen,b   Kurt Hostettmann,b   Orlando Muñoz,c   Sandra Lossd  and  Damien Jeannerat*a  

* Corresponding authors

a Department of Organic Chemistry, University of Geneva, Quai Ernest-Ansermet 30, Geneva 4, Switzerland
E-mail: damien.jeannerat@unige.ch
Fax: +4122 3793215
Tel: +4122 379 6084

b Laboratory of Pharmacognosy and Phytochemistry, School of Pharmaceutical Sciences, University of Geneva, University of Lausanne, Quai Ernest-Ansermet 30, Geneva 4, Switzerland

c Departamento de Química, Facultad de Ciencias, Universidad de Chile, Casilla 653, Santiago, Chile

d Bruker BioSpin AG, Industriestrasse 26, CH-8117 Fällanden, Switzerland

Abstract

The acquisition of a complementary heteronuclear 2D NMR experiment with 10-ppm carbon window allows chemists to improve by a factor 20–25 the spectral resolution and determine carbon chemical shifts with five figures from 2D spectra.

Graphical abstract: High-precision heteronuclear 2D NMR experiments using 10-ppm spectral window to resolve carbon overlap

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Article information

DOI
https://doi.org/10.1039/B820478K
Article type
Communication
Submitted
17 Nov 2008
Accepted
15 Dec 2008
First published
20 Jan 2009

Chem. Commun., 2009, 950-952

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High-precision heteronuclear 2D NMR experiments using 10-ppm spectral window to resolve carbon overlap

B. Vitorge, S. Bieri, M. Humam, P. Christen, K. Hostettmann, O. Muñoz, S. Loss and D. Jeannerat, Chem. Commun., 2009, 950 DOI: 10.1039/B820478K

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