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Issue 5, 2009
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Dynamic kinetic resolution of β-keto sulfones via asymmetric transfer hydrogenation

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Abstract

The dynamic kinetic resolution of β-keto sulfones was achieved via asymmetric transfer hydrogenation using (S,S)-RuCl[N-(tosyl)-1,2-diphenylethylenediamine](p-cymene) in the presence of formic acid and triethylamine afforded the desired products in good yield with up to >99 : 1 dr and high ee up to >99%.

Graphical abstract: Dynamic kinetic resolution of β-keto sulfones via asymmetric transfer hydrogenation

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Publication details

The article was received on 20 Oct 2008, accepted on 26 Nov 2008 and first published on 19 Dec 2008


Article type: Communication
DOI: 10.1039/B818257D
Chem. Commun., 2009, 571-573

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    Dynamic kinetic resolution of β-keto sulfones via asymmetric transfer hydrogenation

    Z. Ding, J. Yang, T. Wang, Z. Shen and Y. Zhang, Chem. Commun., 2009, 571
    DOI: 10.1039/B818257D

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