The syntheses and structures of three cyclophanes containing two (Z)-dehydrophenylalanine residues are reported; the length of the tethers between the two amino acid residues is easily altered and changing this parameter has a significant effect on the solid state structures of the cyclophanes.
S. E. Gibson (née Thomas), J. O. Jones, S. B. Kalindjian, J. D. Knight, J. W. Steed and M. J. Tozer, Chem. Commun., 2002, 1938 DOI: 10.1039/B205752M
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