Issue 17, 2000
From the journal:

Chemical Communications

Dealkylation of a 1,2-bis(benzylthio)benzene derivative: generation of benzodithiete or its equivalent via a dithia dicationElectronic supplementary information (ESI) available: spectral data of compounds. See http://www.rsc.org/suppdata/cc/b0/b004940i/

Kenji Kobayashi,*a   Emiko Koyama,a   Mariko Goto,a   Chikako Nodaa  and  Naomichi Furukawa‡*a  

* Corresponding authors

a Department of Chemistry, University of Tsukuba, Tsukuba, Ibaraki, Japan.
E-mail: kenjinor@staff.chem.tsukuba.ac.jp

Abstract

The reaction of 1,2-bis(4-methylbenzylthio)benzene s-oxide with triflic anhydride in CH3CN–CH2Cl2 in the presence of alkynes affords 1,4-benzodithiin derivatives and N-(4- methylbenzyl)acetamide after quenching with H2O; this suggests the generation of benzodithiete or its equivalent.

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Article information

DOI
https://doi.org/10.1039/B004940I
Article type
Communication
Submitted
20 Jun 2000
Accepted
21 Jul 2000
First published
16 Aug 2000

Chem. Commun., 2000, 1667-1668

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Dealkylation of a 1,2-bis(benzylthio)benzene derivative: generation of benzodithiete or its equivalent via a dithia dication

K. Kobayashi, E. Koyama, M. Goto, C. Noda and N. Furukawa, Chem. Commun., 2000, 1667 DOI: 10.1039/B004940I

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