Issue 13, 2000
From the journal:

Chemical Communications

A novel photocycloaddition of substituted pyridines with benzofuranElectronic supplementary information (ESI) available: experimental section. See http://www.rsc.org/suppdata/cc/b0/b002396p/

Masami Sakamoto,*a   Ai Kinbara,a   Tadao Yagi,a   Takashi Mino,a   Kentaro Yamaguchib  and  Tsutomu Fujitaa  

* Corresponding authors

a Department of Materials Technology, Faculty of Engineering, Chiba University, Yayoi-cho, Inage-ku, Chiba, Japan.
E-mail: saka@galaxy.tc.chiba-u.ac.jp

b Chemical Analysis Center, Chiba University, Yayoi-cho, Inage-ku, Chiba, Japan

Abstract

Irradiation of a benzene solution containing 3-cyano-2-methoxypyridine (0.02 M) and benzofuran (0.5 M) resulted in the formation of stereo-isomeric 1:1 adducts, endo and exo-7-cyano-2-methoxy-4-methyl-9-oxa-3-aza-10,11-benzotricyclo[6. 3.0.04,7]undeca-2,5-diene, accompanied by 5-cyano-2-methoxypyridine and a pyridine dimer; the structures of the adducts were established by X-ray structural analyses.

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Supplementary files

Article information

DOI
https://doi.org/10.1039/B002396P
Article type
Communication
Submitted
27 Mar 2000
Accepted
23 May 2000
First published
15 Jun 2000

Chem. Commun., 2000, 1201-1202

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A novel photocycloaddition of substituted pyridines with benzofuran

M. Sakamoto, A. Kinbara, T. Yagi, T. Mino, K. Yamaguchi and T. Fujita, Chem. Commun., 2000, 1201 DOI: 10.1039/B002396P

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