SCHEDULED MAINTENANCE
The mechanism of the quinone-based palladium-catalysed allylic acetoxylation of cyclohexene is studied using 1,2-dideuteriocyclohexene (55–70% D) as substrate; the distribution of the deuterium label in the product, determined by 1H NMR spectroscopy, is that expected for a (π-allyl)palladium intermediate.
H. Grennberg, V. Simon and Jan-E. Bäckvall, J. Chem. Soc., Chem. Commun., 1994, 265 DOI: 10.1039/C39940000265
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