SCHEDULED MAINTENANCE
Formylphosphonate hydrate 8, synthesized for the first time by the reaction of diethyl diazomethylphosphonate with dimethyl dioxirane (DMD), reacts with primary amines to provide imines 9 and 10; compound 9 is also prepared by the reaction of the anion of diethyl methylenebisphosphonate with nitrosobenzene.
R. Hamilton, M. A. McKervey, M. D. Rafferty and B. J. Walker, J. Chem. Soc., Chem. Commun., 1994, 37 DOI: 10.1039/C39940000037
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