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13 C Labelling and NMR experiments establish the structure of factor IV, the oxidized form of the tetramethylated intermediate on the biosynthetic pathway to precorrin-6x 2 in Pseudomonas denitrificans, thus demonstrating that the contraction of the macrocycle leads to an acetyl derivative at C-1.
D. Thibaut, L. Debussche, D. Fréchet, F. Herman, M. Vuilhorgne and F. Blanche, J. Chem. Soc., Chem. Commun., 1993, 513 DOI: 10.1039/C39930000513
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