SCHEDULED MAINTENANCE
Optically active 2-butenolides with a trifluoromethyl (CF3) group are synthesized via enzymatic optical resolution and are selectively transformed into 6,6,6-trifluororhodinose and amicetose by base-promoted 1,2-migration of a tert-butyldimethylsilyl moiety in a highly efficient manner.
T. Yamazaki, K. Mizutani, M. Takeda and T. Kitazume, J. Chem. Soc., Chem. Commun., 1992, 55 DOI: 10.1039/C39920000055
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