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A convenient, high yield method for the synthesis of ruthenium hydrides, including anionic ruthenium hydrides, has been developed; the molecular structure of potassium trihydridotris(triphenylphosphine)ruthenate (2) complexed with 18-crown-6 ether has been determined by single crystal X-ray diffraction.
A. S. C. Chan and H. Shieh, J. Chem. Soc., Chem. Commun., 1985, 1379 DOI: 10.1039/C39850001379
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