Acyl transfer from acetyl cyanide to either the oxygen of PhNHOH, the nitrogen of MeNHOMe, or the sulphur of PhCH2SH proceeds via tetrahedral intermediates that are readily detected by 1H and 13C n.m.r. spectroscopy.
A. M. Lobo, M. M. Marques, S. Prabhakar and H. S. Rzepa, J. Chem. Soc., Chem. Commun., 1985, 1113 DOI: 10.1039/C39850001113
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