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The structure elucidation of asticolorins A–C, toxic metabolites isolated from cultures of Aspergillus multicolor, is based on X-ray crystallography of asticolorins A (1) and on a betailed study of their 1H and 13C n.m.r. spectra; the chirality of the C-29 Secondary hydroxy group present in asticolorin A, as determined by the method of Horeau, established the absolute configuratgion.
C. J. Rabie, T. J. Simpson, P. S. Steyn, P. H. van Rooyen and R. Vleggaar, J. Chem. Soc., Chem. Commun., 1984, 764 DOI: 10.1039/C39840000764
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