Issue 19, 1980
From the journal:

Journal of the Chemical Society, Chemical Communications

A new synthesis and the X-ray crystal structure of bis(trimethylbenzylammonium) tri-µ-carbonyl-dodecacarbonyl-octahedro-hexairidate(2–)

Francesco Demartin,   Mario Manassero,   Mirella Sansoni,   Luigi Garlaschelli,   Secondo Martinengo  and  Franco Canziani  

Abstract

The [Ir6(CO)15]2– dianion, obtained by a two-step carbonylative reduction of K2IrCl6 in 2-methoxyethanol containing 10% of water, has been shown by X-ray diffraction to contain an octahedral Ir6 cluster with twelve terminal and three symmetrical edge-bridging carbonyl groups.

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Article information

DOI
https://doi.org/10.1039/C39800000903
Article type
Paper

J. Chem. Soc., Chem. Commun., 1980, 903-904

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A new synthesis and the X-ray crystal structure of bis(trimethylbenzylammonium) tri-µ-carbonyl-dodecacarbonyl-octahedro-hexairidate(2–)

F. Demartin, M. Manassero, M. Sansoni, L. Garlaschelli, S. Martinengo and F. Canziani, J. Chem. Soc., Chem. Commun., 1980, 903 DOI: 10.1039/C39800000903

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