Issue 21, 1973
From the journal:

Journal of the Chemical Society, Chemical Communications

Preparation and nuclear magnetic resonance parameters of perfluoroalkyl-substituted phosphorus(V) hydrides

John W. Gilje,   Ronald W. Braun  and  Alan H. Cowley  

Abstract

The phosphorus(V) hydrides (CF3)3PH2(1), CF3PF3H (2), and (CF3)2PF2H (3) have been prepared by the vapour phase reaction of the appropriate fluorophosphorane, (CF3)nPF5–n, with Me3SiH; the labile dihydride, CF3PF2H2(4) was detected in the (reversible) liquid phase reaction of CF3PF4 with Me3SiH.

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Article information

DOI
https://doi.org/10.1039/C39730000813
Article type
Paper

J. Chem. Soc., Chem. Commun., 1973, 813-814

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Preparation and nuclear magnetic resonance parameters of perfluoroalkyl-substituted phosphorus(V) hydrides

J. W. Gilje, R. W. Braun and A. H. Cowley, J. Chem. Soc., Chem. Commun., 1973, 813 DOI: 10.1039/C39730000813

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