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The crystal structure of the adduct Fe(NO3)3,–1·5N2O4 indicates that it should be represented as 3NO+,NO3–,2[Fe(NO3)4–]; vibrational spectroscopy provides evidence for interaction between the NO3– and 3NO+ ions, and the properties are correlated in terms of a weakly bonded N4O62+ group which may also be present in solutions of N2O4, or the adduct, in pure nitric acid.
C. C. Addison, L. J. Blackwell, B. Harrison, D. H. Jones, N. Logan, E. K. Nunn and S. C. Wallwork, J. Chem. Soc., Chem. Commun., 1973, 347 DOI: 10.1039/C39730000347
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