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Issue 20, 2013
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Expedient preparative isolation, quantification and characterization of limonoids from Neem fruits

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Abstract

Major basic limonoids from Neem fruits such as azadirone, epoxyazadiradione and azadiradione were isolated in preparative scale using an automated and rapid medium pressure liquid chromatography (MPLC)-based protocol. They were individually quantified using HPLC. An LC-ESI-MS/MS-based rapid identification technique was developed for the high-throughput screening of these limonoids in phytochemical extracts.

Graphical abstract: Expedient preparative isolation, quantification and characterization of limonoids from Neem fruits

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Article information


Submitted
09 Jul 2013
Accepted
24 Aug 2013
First published
28 Aug 2013

Anal. Methods, 2013,5, 5386-5391
Article type
Communication

Expedient preparative isolation, quantification and characterization of limonoids from Neem fruits

S. Haldar, P. B. Phapale, S. P. Kolet and H. V. Thulasiram, Anal. Methods, 2013, 5, 5386
DOI: 10.1039/C3AY41136B

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