Issue 10, 2012
From the journal:

Analytical Methods

Detection of intermediates in Leuckart reaction by desorption corona beam ionization ambient mass spectrometry

Guangming Xu,ac   Bo Chen,*b   Hua Wang,b   Yinzhuang Chen,a   Li Dingd  and  Shouzhuo Yao*a  

* Corresponding authors

a State Key Laboratory of Chemo/Biosensing and chemometrics, College of Chemistry and Chemical Engineering, Hunan University, Changsha 410081, China
E-mail: Yasz@yahoo.com.cn
Fax: +86 731 8865515
Tel: +86 731 8865515

b Key Laboratory of Chemical Biology and Traditional Chinese Medicine Research (Ministry of Education of China), Hunan Normal University, Changsha 410081, China
E-mail: dr-chenpo@vip.sina.com
Fax: +86 731 8865515
Tel: +86 731 8865515

c College of Pharmaceutical Science of Hunan University of Chinese Medicine, Changsha 410208, China

d Shimadzu Research Laboratory (Shanghai) Co., Ltd, Shanghai, China

Abstract

Desorption corona beam ionization mass spectrometry, a novel direct MS analysis technique, was first employed to probe intermediates in Leuckart reaction between ketone and ammonium formate at 185 °C to corroborate the reaction mechanism.

Graphical abstract: Detection of intermediates in Leuckart reaction by desorption corona beam ionization ambient mass spectrometry

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Article information

DOI
https://doi.org/10.1039/C2AY25588J
Article type
Communication
Submitted
07 Jun 2012
Accepted
15 Aug 2012
First published
16 Aug 2012

Anal. Methods, 2012,4, 3098-3101

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Detection of intermediates in Leuckart reaction by desorption corona beam ionization ambient mass spectrometry

G. Xu, B. Chen, H. Wang, Y. Chen, L. Ding and S. Yao, Anal. Methods, 2012, 4, 3098 DOI: 10.1039/C2AY25588J

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